Wittig Reagent

This derivative of triphenylphosphine is the main reagent in the second step of the synthesis, known as the Wittig Reaction. The reagent is prepared by dissolving Ph3PCH3 in THF and n-BuLi, which deprotonates the methyl group and forms a methylene group. This reacts with the ketone carbon on the original molecule, forming a cyclic transition state in the process, in order to reduce the ketone to a methylene group.

General Wittig Reagent