While the report of a 67-year-old Florida woman shoplifting in a turkey costume have been confirmed, said crime spree most likely did not take place in the experimental section.
A solution of (±)-12 (10.0 mg, 0.0342 mmol) in CH3OH (0.5 mL) was treated with a catalytic amount of NaH at 22 ˚C, and stirred for 4 h at 22 ˚C. sat. NH4Cl aq. was added and the resulting mixture was extracted with CH2Cl2 (2 times) and the combined organic layers were dried over Na2SO4, filtered and concentrated in vacuo. The residue was purified by preparative TLC (hexanes/acetone = 1:1) to provide (±)-15 as a white solid (9.0 mg, 81%).
Ohtawa, M.; Krambis, M.; Cerne, R.; Schkeryantz, J.; Witkin, J.; Shenvi, R. J. Am. Chem. Soc. 2017, 139, 9637-9644.